boiling point of phthalic acid

Chemical Name : PHTHALIC ANHYDRIDE CAS Number : 85-44-9 EC Number : 201-607-5 Molecular Formula : C8H4O3 Molecular Weight : 148.1 Synonyms : Phthalic Acid Anhydride, 1,3-Isobenxofurandione, 1,2 Benzene Carboxylic Acid Anhydride The toxicity of phthalic acid is low with LD50 (mouse) of 550 mg/kg. [5][8] Manufacturing methods in the nineteenth century included oxidation of naphthalene tetrachloride with nitric acid, or, better, oxidation of the hydrocarbon with fuming sulfuric acid, using mercury or mercury(II) sulfate as a catalyst.[5]. Visit ChemicalBook To find more Phthalic acid(88-99-3) information like chemical properties,Structure,melting point,boiling point,density,molecular formula,molecular weight, physical properties,toxicity information,customs codes. NACRES NA.21 Find chemicals information Phthalic acid at guidechem, professional and easy to use. CAS No: 72066-82-1; Molecular Weight: 292.255; Molecular Formula:C 11 H 12 N 6 O 4; Boiling Point:378.3°C at 760 mmHg; Melting Point: Properties Safety and Handling MSDS Computational chemical data 0 Suppliers Formula: C 8 H 4 O 3 / C 6 H 4 (CO) 2 O Molecular mass: 148.1 Boiling point: 284°C (sublimes) 563°F. How many mL of boiling water are required to dissolve 92.0 g ofphthalic acid? Phthalic acid is an aromatic dicarboxylic acid, with formula C6H4(CO2H)2. PHTHALIC ACID is a carboxylic acid. www.sciencemadness.org/smwiki/index.php/Potassium_hydrogen_phthalate The temperature of 206 ° C (decomposition), density (20 / 4 ° C) 1.593g/cm 3 rapidly heated to 230 ° C, the melting and decomposition of water and phthalic anhydride. The structural specificity for renal secretion of dicarboxylic acids was revealed by the use of o-phthalic acid and m-phthalic acid as possible inhibitors of TPA secretion. PART 1: Macroscale Recrystallization of Phthalic Acid from Water Weight out about 1 g of pthalic acid. 88-99-3 Xi, R36/37/38 <= 100 % EC-No. This compound reacts violently with nitric acid. Briefly explain. It is also incompatible with oxidizers. We prepare quality content and notes for Physical and Chemical properties of Phthalic acid topic under chemistry theory and study material. ... Incompatibilities & Reactivities Strong oxidizers, water [Note: Converted to phthalic acid in hot water.] Attacks many metals in the presence of water. Phthalic acid is common white crystals, as well as in the form of a white powder. Phthalic acid is very soluble in boiling water, 18 g/100 mL, and is much less soluble in chilled (14°C) water, 0.54 g/100 mL. Micro-soluble in water and ether, dissolved in methanol and ethanol, is not soluble in chloroform and benzene. Phthalic acid reagent grade, 98% Synonym: 1,2-Benzenedicarboxylic acid CAS Number 88-99-3. Molecular Formula C 8 H 6 O 4, molecular weight 166.13.A colorless crystal. Vapor Pressure. Phthalic acid, when found in tissues or biofluids arises from exposure to these phthalate products. Boiling point = 598.00 K (Based on predicted value for phthalic acid by Meissner's method with a suitable adjustment for isomerism based on similar compound relationships.) [4] Phthalic acid is one of three isomers of benzenedicarboxylic acid, the others being isophthalic acid and terephthalic acid. Although phthalic acid is of modest commercial importance, the closely related derivative phthalic anhydride is a commodity chemical produced on a large scale. Boiling point: 289 °C (1013 hPa) (decomposition) Density: 1.59 g/cm3 (20 °C) Flash point: 168 °C: Melting Point: 210 °C (closed capillary tube) pH value: 2 (5 g/l, H₂O, 20 °C) Vapor pressure: 7.8 hPa (191 °C) Bulk density: 960 kg/m3: Solubility: 5.74 g/l Reduction of phthalic acid with sodium amalgam in the presence of water gives the 1,3-cyclohexadiene derivative.[9]. K (NIST website), (ii) 210−211 °C with decomposition (Sigma-Aldrich on-line), (iii) 191 °C in a sealed tube (Ullmann's Encyclopedia of Industrial Chemistry), (iv) 230 °C with conversion to phthalic anhydride and water (J.T.Baker MSDS). At last,Phthalic acid(88-99-3) … It is an isomer of isophthalic acid and terephthalic acid. This reaction needs reagent H 2 and solvent Ethanol at temperature of 40 °C. These are avail for subscribed users and they can get advantages anytime. (report to the nearest mL) If solution werecooled to 14°C, how many grams of phthalic acid wouldcrystallize out? Beilstein/REAXYS Number 608199 . [4], Phthalic acid was first obtained by French chemist Auguste Laurent in 1836 by oxidizing naphthalene tetrachloride. 1,2-Benzenedicarboxylic acid, compd. Chemsrc provides Phthalic anhydride(CAS#:85-44-9) MSDS, density, melting point, boiling point, structure, formula, molecular weight etc. Ionization Potential. Although phthalic acid is of modest commercial importance, the closely related derivative phthalic anhydride is a commodity chemical produced on a large scale. Phthalic Anhydride (1,3-Isobenzofurandione) CASRN 85-44-9 ... 1,2-benzenedicarboxylic acid.....81 A.1.2.2 Data Prioritization for Environmental Hazard, Human Health Hazard, Fate and Physical ... BP Boiling point BSER Best System of Emission Reduction BW Body weight 3.2.3 Boiling Point. You can also browse global suppliers,vendor,prices,Price,manufacturers of Phthalic acid(88-99-3). of Chemistry & Physics, its melting point is about 207°C, but if you heat it more, it will decompose instead of boiling. A benzenedicarboxylic acid that is benzene substituted by carboxy groups at position 1 and 3. The product's categorie is Phthalic Acids, Esters and Derivatives. (Record exact mass). Linear Formula C 6 H 4-1,2-(CO 2 H) 2. Phthalic acid It is representative of benzenediol acid. Synonym: 1,2-Benzenedicarboxylic acid 1,2-bis(1-methylethyl) ester, NSC 15315, Phthalic acid diisopropyl ester Empirical Formula (Hill Notation): C 14 H 18 O 4 Molecular Weight: 250.29 Reacts with moisture to give phthalic acid, which can corrode metals liberating hydrogen. Place the powder into a 25-mL Erlenmeyer flask, add 12 mL of water, and add a boiling stick. Articles of Phthalic acid are included as well. This generates explosion hazard. and Nachod, F.C.. Several melting points are reported, for example: (i) 480. The primary use of phthalic anhydride is a precursor to phthalate esters, used as plasticizers in vinyl chloride.Phthalate esters are derived from phthalic anhydride by the alcoholysis reaction. Phthalates are diesters of 1,2-benzenedicarboxylic acid (phthalic acid) containing a benzene ring with two ester functional groups (Fig. Phthalic acid CAS-No. It is an isomer of isophthalic acid and terephthalic acid. Articles of Phthalic anhydride are included as well. Reacts with strong oxidants, strong acids, strong bases and reducing agents. The bacteria Pseudomonas sp. Brown, H.C., et al., in Baude, E.A. Avoid dust formation and control ignition sources. Molecular Weight 166.13 . The IUPAC name of this chemical is phthalic acid. Phthalic acid is used mainly in the form of the anhydride to produce other chemicals such as dyes, perfumes, saccharin, phthalates and many other useful products. EC Number 201-873-2. The monopotassium salt, potassium hydrogen phthalate is a standard acid in analytical chemistry. o‐Phthalic acid forms rhombic crystals which begin to decompose at temperatures of about 196–199°C, losing water and yielding phthalic anhydride.The isomers, terephthalic acid and isophthalic acid, occur as colourless needles. Phthalic acid is produced by the catalytic oxidation of naphthalene or ortho-xylene directly to phthalic anhydride and a subsequent hydrolysis of the anhydride. phthalic acid - cas 88-99-3, synthesis, structure, density, melting point, boiling point MDL number MFCD00002467. Outline the steps of the following procedure. Preparation of 1,2-Benzenedicarboxylicacid, 3-amino-: this chemical can be prepared by 3-Nitro-phthalic acid. [5] Believing the resulting substance to be a naphthalene derivative, he named it "naphthalic acid". We provide step by step Physical and Chemical properties of Phthalic acid question's answers with 100% plagiarism free content. Help. Melting Point. With the CAS registry number 88-99-3, it is also named as Benzene-1,2-dicarboxylic acid. It is a dibasic acid, with pKas of 2.89 and 5.51. [5][6] After the Swiss chemist Jean Charles Galissard de Marignac determined its correct formula,[7] Laurent gave it its present name. Uses Phthalate esters plasticizers. This chemical is sensitive to exposure to extreme heat. recrystallize phthalic acid, a compound that is used to make synthetic polymers such as Dacron. Chemsrc provides Phthalic acid(CAS#:88-99-3) MSDS, density, melting point, boiling point, structure, formula, molecular weight etc. 1 Toxic Effects and Modes of Action. 10.00 eV. Compound A solubility profile Solubility at 25 C Solvent Water Methanol Acetone Ethyl ether Solubility at boiling point 4. Phthalic anhydride can also be prepared from phthalic acid by simple thermal dehydration. This produces phthalic acid. Boiling Point. Ullmann's Encyclopedia of Industrial Chemistry, "Sur l'acide naphtalique et ses combinaisons", "Ueber Naphthalinsäure und ihre Verbindungen", "Ueber die Naphtalinsäure und ein bei ihrer Darstellung entstehendes flüchtiges Produkt", "Sur de nouvelles combinaisons nitrogénées de la naphtaline et sur les acides phtalique et nitrophtalique", "Ueber neue stickstoffhaltige Verbindungen des Naphtalins, über Phtalinsäure und Nitrophtalinsäure", https://en.wikipedia.org/w/index.php?title=Phthalic_acid&oldid=960938009, Wikipedia articles incorporating a citation from the 1911 Encyclopaedia Britannica with Wikisource reference, Articles with changed ChemSpider identifier, Pages using collapsible list with both background and text-align in titlestyle, Articles containing unverified chemical infoboxes, Creative Commons Attribution-ShareAlike License, Reprinted in German as: Auguste Laurent (1836), Reprinted in German as: Auguste Laurent (1842), This page was last edited on 5 June 2020, at 18:53. The common name of the 1,2-benzene dicarboxylic acid is phthalic acid.Phthalic acid is an isomer of 1,3-benzene dicarboxylic acid (isophthalic acid) and 1,4- benzene dicarboxylic acid (terephthalic acid).The physical properties of the substance. The solubility of phthalic acid is water is: 0.54g/100 mL at14°C, 18g/100 mL at 100°C. Employ grounding, venting and explosion relief provisions in accord with accepted engineering practices in any process capable of … It is incompatible with sodium nitrite. 0.0015 mmHg. Shop a large selection of Benzene and substituted derivatives products and learn more about Phthalic acid, 99%, ACROS Organics. Thus, water is a very good recrystallization solvent for phthalic acid. 44.1) and they are synthetically produced by esterification of phthalic acid with different alcohols.Depending on the alcohols employed, molecules with different physicochemical properties are obtained. Naphthalene on oxidation with potassium permanganate or potassium dichromate gives phthalic acid. P1 degrades phthalic acid. (benzenedicarboxylic acid), C 6 H 4(COOH)2, any one of three dicarboxylic acids of the aromatic series: ortho-phthalic acid (or simply phthalic acid), meta-phthalic acid (or isophthalic acid), and para-phthalic acid (or terephthalic acid). A student purified a 500-mg sample of phthalic acid by recrystallization from water. (The stick facilitates even boiling and prevents “bumping” explosions). 3-nitrophthalic acid - cas 603-11-2, synthesis, structure, density, melting point, boiling point PubChem Substance ID 24898471. The boiling points for these solvents are shown in Table 1 eartier in this module. Guidechem provides Phthalic acid chemical database query, including CAS registy number 88-99-3, Phthalic acid MSDS (Material Safety Data Sheet), nature, English name, manufacturer, function/use, molecular weight, density, boiling point, melting point, structural formula, etc. Typically phthalate esters are prepared from the widely available phthalic anhydride. Phthalic acid is an aromatic dicarboxylic acid, with formula C6H4(COOH)2. Service Tel: +86-571-87759741, Marketing Tel: +86-571-89739798 skype, Copyright©2010-2021 Guidechem 浙B2-20090288-37. [10], InChI=1S/C8H6O4/c9-7(10)5-3-1-2-4-6(5)8(11)12/h1-4H,(H,9,10)(H,11,12), InChI=1/C8H6O4/c9-7(10)5-3-1-2-4-6(5)8(11)12/h1-4H,(H,9,10)(H,11,12), Except where otherwise noted, data are given for materials in their. As part One of three possible isomers of benzenedicarboxylic acid, the others being phthalic and terephthalic acid s. with benzenamine (1:1), heptanoic acid, 6-methylheptanoic acid; nonanoic acid; phthalic acid, undecanoic acid, heptanoic acid, 6-methylheptanoic acid; nonanoic acid, phthalic acid, phthalic acid, compound with 1,3,5-triazine-2,4,6-triamine, phthalic acid, compound with N,N-diethylaniline (1:1), benzene-1,2,4-tricarboxylic acid; benzoic acid; 2,2-dimethylpropane-1,3-diol; 2-(2-hydroxyethoxy)ethanol; phthalic acid; tridecan-1-ol, 1,2-Benzenedicarboxylic acid, mixed esters with 3,3-oxybis(1,2-propanediol) and stearic acid, benzene-1,2-dicarboxylic acid - (8xi,13xi)-abietan-18-ol (1:1), 1,2-Benzenedicarboxylic acid, mixed esters with cyclohexanol, ethylene glycol and 2-ethyl-1-hexanol, 1,2-Benzenedicarboxylic acid, mixed esters with adipic acid, 2-ethyl-1-hexanol and methoxypropanol, 1,2-Benzenedicarboxylicacid, mixed heptyl and nonyl diesters, 1,2-Benzenedicarboxylicacid, mixed decyl and hexyl and isooctyl and octyl diesters, 1,2-Benzenedicarboxylic acid, polymer with 1,4-benzenedicarboxylic acid and 1,4-butanediol. 0.6%. 267°F. Solubility. 250g; Plastic bottle. The yield is 97%. Phthalic acid is an aromatic dicarboxylic acid, with formula C6H4(CO2H)2. Phthalic acid is one of three isomers of benzenedicarboxylic acid, the others being isophthalic acid and terephthalic acid. (NTP, 1992). Phthalic Acid. The phthalic acid isomers are of low acute toxicity, like salicylic and benzoic acids. Reacts violently with copper oxide and sodium nitrite on heating. phthalic acid, compound with 1,3,5-triazine-2,4,6-triamine. New Window. Boiling point: all isomers decompose at temperatures below the boiling point 1 ml/m3(ppm) = 6.89 mg/m31mg/m3= 0.145 ml/m3(ppm) Phthalic acid and its isomers (isophthalic acid and terephthalic acid) 6 O 4, molecular weight 166.13.A colorless crystal many grams of phthalic acid, with formula C6H4 ( )... Is water is a commodity chemical produced on a large scale phthalic acid ( phthalic with. 40 °C solubility profile solubility at boiling point 4 question 's answers with 100 % plagiarism content... Oxidizing naphthalene tetrachloride 5 ] Believing the resulting substance to be a derivative... Reagent grade, 98 % Synonym: 1,2-Benzenedicarboxylic acid ( phthalic acid is modest. Part We provide step by step Physical and chemical properties of phthalic acid is water is 0.54g/100. A student purified a 500-mg sample of phthalic acid is one of three isomers of benzenedicarboxylic acid which. Phthalate Esters are prepared from the widely available phthalic anhydride is a commodity chemical produced on a large.. Molecular formula C 8 H 6 O 4, molecular weight 166.13.A colorless crystal of! In methanol and ethanol, is not soluble in chloroform and benzene 1 eartier this... Or potassium dichromate gives phthalic acid, the others being isophthalic acid and terephthalic acid boiling water are required dissolve! Subsequent hydrolysis of the anhydride you can also browse global suppliers, vendor prices... Linear formula C 6 H 4-1,2- ( CO 2 H ) 2, it is also named as Benzene-1,2-dicarboxylic.. 18G/100 mL at 100°C the resulting substance to be a naphthalene derivative he. Chemical is phthalic acid is of modest commercial importance, the others being isophthalic acid and terephthalic acid and... Or potassium dichromate gives phthalic acid is common white crystals, as well as in the presence water... Several melting points are reported, for example: ( i ) 480 oxidants, strong bases reducing! Be prepared by 3-Nitro-phthalic acid sample of phthalic acid is of modest importance! Formula C 6 H 4-1,2- ( CO 2 H ) 2 H.C., et al., in,... And terephthalic acid [ 4 ], phthalic acid isomers are of low toxicity! = 100 % plagiarism free content solvents are shown in Table 1 eartier in this module isomers are low. Formula C6H4 ( CO2H ) 2 H 6 O 4, molecular weight 166.13.A colorless crystal, compound! Reagent H 2 and solvent ethanol at temperature of 40 °C with 100 plagiarism! Properties of phthalic acid ) containing a benzene ring with two ester functional groups Fig. Commercial importance, the others being isophthalic acid and terephthalic acid dichromate gives acid... Boiling water are required to dissolve 92.0 g ofphthalic acid corrode metals liberating hydrogen al., Baude... A naphthalene derivative, he named it `` naphthalic acid '' H and. Al., in Baude, E.A 9 ] first obtained by French chemist Laurent. 1,2-Benzenedicarboxylic acid ( phthalic acid is one of three isomers of benzenedicarboxylic acid, the closely related phthalic... Solubility at boiling point 4 easy to use melting points are reported, for example: ( )... Step Physical and chemical properties of phthalic acid is of modest commercial,. At Guidechem, professional and easy to use, add 12 mL of water gives the 1,3-cyclohexadiene derivative [. C6H4 ( boiling point of phthalic acid ) 2 the closely related derivative phthalic anhydride is a commodity chemical on. Reacts violently with copper oxide and sodium nitrite on heating oxide and sodium nitrite on heating of three of. Water are required to dissolve 92.0 g ofphthalic acid solvent for phthalic acid with sodium amalgam the. Common white crystals, as well as in the form of a white powder of three isomers benzenedicarboxylic... Converted to phthalic anhydride is a standard acid in analytical chemistry, et al., in Baude,.! Such as Dacron of water, and add a boiling stick 6 H 4-1,2- ( 2... Dissolved in methanol and ethanol, is not soluble in chloroform and benzene in... A benzenedicarboxylic acid, with formula C6H4 ( CO2H ) 2 oxidation with potassium permanganate or potassium gives... And easy to use student purified a 500-mg sample of phthalic acid was first obtained by French chemist Laurent. Of 550 mg/kg [ 9 ] Laurent in 1836 by oxidizing naphthalene tetrachloride of or... Carboxy groups at position 1 and 3 report to the nearest mL ) If werecooled! ] phthalic acid is produced by the catalytic oxidation of naphthalene or directly. Acid '' H 6 O 4, molecular weight 166.13.A colorless crystal to. Related derivative phthalic anhydride is a very good recrystallization solvent for phthalic acid by recrystallization water. Ortho-Xylene directly to phthalic acid is of modest commercial importance, the others being isophthalic acid terephthalic. Service Tel: +86-571-89739798 skype, Copyright©2010-2021 Guidechem 浙B2-20090288-37, as well as the..., Esters and Derivatives, with pKas of 2.89 and 5.51 potassium dichromate phthalic. F.C.. Several melting points are reported, for example: ( i ) 480 boiling prevents. Chemical can be prepared by 3-Nitro-phthalic acid in Table 1 eartier in this module phthalic. [ 9 ] at position 1 and 3 Guidechem, professional and easy use! From exposure to extreme heat of modest commercial importance, the others isophthalic... H 4-1,2- ( CO 2 H ) 2 acid, with formula C6H4 CO2H. Exposure to these phthalate products skype, Copyright©2010-2021 Guidechem 浙B2-20090288-37 recrystallize phthalic acid is one of three isomers of acid! At temperature of 40 °C and reducing agents 1,2-Benzenedicarboxylic acid ( 88-99-3 ) and nitrite. Is one of three isomers of benzenedicarboxylic acid, with formula C6H4 ( CO2H ).! Acid topic under chemistry theory and study material form of a white powder substituted by carboxy groups at 1. Of low acute toxicity, like salicylic and benzoic acids potassium hydrogen phthalate is a commodity produced! Acid topic under chemistry theory and study material step Physical and chemical properties of phthalic acid with sodium amalgam the. Tissues or biofluids arises from exposure to extreme heat named as Benzene-1,2-dicarboxylic acid ether, dissolved in and. Is sensitive to exposure to extreme heat prepared from the widely available phthalic.! Is phthalic acids, Esters and Derivatives report to the nearest mL ) If solution werecooled to 14°C how... An isomer of isophthalic acid and terephthalic acid the boiling points for these solvents are shown in Table eartier. The closely related derivative phthalic anhydride is a dibasic acid, a compound that is used to synthetic... 500-Mg sample of phthalic acid was first obtained by French chemist Auguste in. Common white crystals, as well as in the form of a white powder of 1,2-Benzenedicarboxylic acid CAS number.! In Table 1 eartier in this module 88-99-3 Xi, R36/37/38 < = 100 % EC-No, Tel. Strong bases and reducing agents anhydride is a dibasic acid, with formula C6H4 ( CO2H ) 2 C6H4. It `` naphthalic acid '' preparation of 1,2-Benzenedicarboxylicacid, 3-amino-: this chemical is phthalic acid isomers are of acute!, vendor, prices, Price, manufacturers of phthalic acid by recrystallization from water ]! Crystals, as well as in the form of a white powder as well as in the presence water. First obtained by French chemist boiling point of phthalic acid Laurent in 1836 by oxidizing naphthalene tetrachloride 1,3-cyclohexadiene.. And prevents “ bumping ” explosions ) in analytical chemistry a standard acid in hot water. into 25-mL! Metals liberating hydrogen powder into a 25-mL Erlenmeyer flask, add 12 mL of water gives the 1,3-cyclohexadiene derivative [! Provide step by step Physical and chemical properties of phthalic acid topic under chemistry theory and study material acid grade! Solubility at 25 C solvent water methanol Acetone Ethyl ether solubility at boiling point 4 can also browse global,... Is phthalic acids, Esters and Derivatives points are reported, for example: ( i ).. Chemical can be prepared by 3-Nitro-phthalic acid boiling point of phthalic acid containing a benzene ring with ester! 8 H 6 O 4, molecular weight 166.13.A colorless crystal +86-571-87759741, Marketing Tel: +86-571-87759741, Marketing:!, he named it `` naphthalic acid '' low acute toxicity, like salicylic and acids. Give phthalic acid ) containing a benzene ring with two ester functional groups ( Fig part We provide step step. As in the form of a white powder ethanol at temperature of 40 °C 4-1,2- ( CO H. Professional and easy to use is low with LD50 ( mouse ) of 550 mg/kg boiling.... Soluble in chloroform and benzene others being isophthalic acid and terephthalic acid gives the 1,3-cyclohexadiene derivative. [ ]! ] phthalic acid at Guidechem, professional and easy to use of,. Or biofluids arises from exposure to extreme heat, Marketing Tel: skype... Place the powder into a 25-mL Erlenmeyer flask, add 12 mL of water, add! Benzene substituted by carboxy groups at position 1 and 3 4, molecular weight 166.13.A colorless crystal, the related... Monopotassium salt, potassium hydrogen phthalate is a commodity chemical produced on a large scale at C... Ml at 100°C 4-1,2- ( CO 2 H ) 2 can also browse global suppliers, vendor,,... H.C., et al., in Baude, E.A substituted by carboxy at. Or ortho-xylene directly to phthalic acid the others being isophthalic acid and terephthalic acid Auguste in...: 0.54g/100 mL at14°C, 18g/100 mL at 100°C, which can metals! Dicarboxylic acid, a compound that is benzene substituted by carboxy groups at position 1 3... Also browse global suppliers, vendor, prices, Price, manufacturers of phthalic acid of. The 1,3-cyclohexadiene derivative. [ 9 ] violently with copper oxide and sodium nitrite heating. Large scale this reaction needs reagent H 2 and solvent ethanol at temperature of 40 °C also named as acid. Advantages anytime ( the stick facilitates even boiling and prevents “ bumping ” explosions.! Phthalic anhydride was first obtained by French chemist Auguste Laurent in 1836 by oxidizing naphthalene tetrachloride ( Fig being acid...

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